How do I make an equimolar pool for sequencing?

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When preparing sequencing-ready libraries, it is important to create an equimolar pool so that each library contributes equally to the final sequencing run. Below is the recommended workflow using the CUTANATM CUT&RUN Library Prep Kit (EpiCypher 14-1001).

  1. Quantify each library and assess library size

    • Calculate the concentration of each library using the 200 - 700 bp range on the Agilent TapeStation® or Bioanalyzer®. Note that in most cases you will need to manually set this window.

    • Record the average fragment size (in base pairs) as determined by the TapeStation/BioAnalyzer.

  2. Calculate molar concentration

    • Convert concentration (ng/µL) into molarity (nM) using the following formula (where 660 g/mol/bp is the approximate molecular weight of double-stranded DNA):

nM = (concentration in ng/µL × 1,000,000) ÷ (660 × average fragment size in bp)

  1. Normalize libraries

    • Dilute each library to a common molarity using nuclease-free water or a low-EDTA buffer (such as 0.1X TE).

  2. Pool normalized libraries

    • Combine equal volumes (e.g., 5 µL) of each normalized library into a single tube. This creates the equimolar pool.

  3. Validate pooled libraries

    • Run the pool on a TapeStation or Bioanalyzer to confirm pooled fragment distribution. If needed, perform clean up for small fragments on the entire pooled library at this time.

    • Quantify the pool using Qubit.

  4. Dilute to the concentration required for your sequencing platform.

Key Notes

  • Always normalize based on molarity, not mass concentration, to ensure equal sequencing representation.

  • If libraries vary widely in concentration, do NOT dilute to the lowest concentration sample.